MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\CPK\\CPK2017-216-05946-1.D Tgt Mass (EZX): 409.60 Injection Date : 16 Feb 17 3:26 pm +0800 Seq. Line : 0 Sample Name : CPK2017-216-05946-1 Location : P2-A-02 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 4 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-12063 Batch#05946 Easy-Access Method: '1-POS-3MIN' 409.60 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 B, Sig=214,4 Ref=off mAU75050025000.5*DAD1 C, Sig=254,4 Ref=off mAU7500.8471.6581.8341.9422.12650025002.2372.3452.4492.5790.8471.3711.4621.5381.6912.12611.522.52.579min*0.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701500001000005000001.522.52.590min*0.511.5 Ion 410.6, MSD1 410.6,Target Mass 409.6 +H Positive, EIC=410.3:411.3 4000030000200001000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.52.550min22.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.85 0.03 50.08 24.32 1.78 ND 1.37 0.03 3.30 1.67 0.12 701 1.46 0.03 4.56 2.58 0.16 143 1.54 0.03 15.11 0.17 0.54 274 1.69 0.03 2.01 0.47 0.07 141 2.13 0.02 4.56 3.08 0.16 233 2.58 0.04 2735.15 1215.03 97.17 410 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.85 0.03 6.76 3.09 0.25 ND 1.66 0.07 3.37 0.81 0.12 141 1.83 0.03 0.66 0.37 0.02 141 1.94 0.04 2.42 0.90 0.09 233 2.13 0.02 17.45 10.78 0.63 233 2.24 0.03 2.25 1.20 0.08 233 2.35 0.03 6.17 2.62 0.22 141HY-LCMS-02 2/16/2017 3:48:31 PM GZZ_718Page 1 of 3
MS Report from Instrument: HY-LCMS-02
2.45 0.04 9.30 3.58 0.34 141 2.58 0.04 2706.54 1186.93 98.24 410HY-LCMS-02 2/16/2017 3:48:31 PM GZZ_718Page 2 of 3
MS Report from Instrument: HY-LCMS-02
Ret. Time: 2.59 <<<< POSITIVE SPECTRA >>>> ES-API Positive2500020000150001000050000200300400500600700800900m/z 410.3 141.2 233.3 338.4 412.1 819.4HY-LCMS-02 2/16/2017 3:48:31 PM GZZ_718
433.3 473.3 842.3Page 3 of 3
