MS Report File ..0141231 2014-12-31 09-27-51\\XJW2233-045-1.D Tgt Mass (CHM): Injection Date : 31 Dec 14 10:13 am +0800 Seq. Line : 10 Sample Name : XJW2233-045-1 Location : Vial 11 Acq. Operator : Li Shan(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\\Aglient 1260\\Data\\20141231\\20141231 2014-12-31 09-27-51\\100-1000MS+3MIN( Analysis Method : D:\\AGLIENT 1260\\DATA\\20141230\\20141230 2014-12-30 09-01-41\\100-1000MS+3MIN( Catalog No : HY-15954 Batch#14485 A-RP-32 Method Info : Postive,MS:100-1000,Column ID:A-RP-102,40℃ DAD1 B, Sig=214,4 Ref=off 20001500100050000.5 DAD1 C, Sig=254,4 Ref=off mAU100075050025000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 50100000080000060000040000020000000.51 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.7 0.050-0.050.5 Integration Results for DAD1 B, Sig=214,4 Ref=off-0.111.522.53min1.511.51.7091.7111.832mAU2.26022.53min1.5021.8321.51.7501.80322.53min22.53min RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.71 0.08 12528.63 2604.39 85.85 1.83 0.13 2043.83 267.58 14.01 2.26 0.06 20.36 5.27 0.14 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.50 0.08 5.92 1.31 0.10 1.71 0.05 5437.02 1355.09 88.57 1.83 0.13 695.57 87.23 11.33HY-LCMS-02 12/31/2014 11:27:07 AM Li Shan(LCMS-02)Page 1 of 2
MS ReportRet. Time: 1.75 <<<< POSITIVE SPECTRA >>>> ES-API Positive 330.3 659.3Ret. Time: 1.80 ES-API Positive350000300000250000200000 330.2 330.91600001400001200001000008000060000 661.3150000 661.3 659.3 662.340000200000200400600 313.3100000500000800m/z200400600m/zHY-LCMS-02 12/31/2014 11:27:07 AM Li Shan(LCMS-02)Page 2 of 2
