MS Report from Instrument: LCMS-03 File ..\\2018\\20180816\\20180816\\CPK2018-816-16869.D Tgt Mass (CHM): Injection Date : 16 Aug 18 1:41 pm +0800 Seq. Line : 44 Sample Name : CPK2018-816-16869 Location : P1-D-07 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\2018\\20180816\\20180816\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\2018\\20180816\\20180816\\1-POS-3MIN.M Catalog No : HY-16965 Batch#16869 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off10000.986500000.5 DAD1 B, Sig=254,4 Ref=offmAU0.975200000.5 ELS1 A, ELSD SignalmV1.362151000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701500000100000050000001.3011.276mAU1.4801.5471.5921.71211.2751.522.5min1.5521.5931.4811.71211.522.5min1.522.5min1.03200.51 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.70.050-0.05-0.100.511.522.5min1.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.99 0.02 18.53 -0.33 0.84 159 1.28 0.02 2186.08 1665.65 98.79 269 1.48 0.02 0.63 0.60 0.03 269 1.55 0.02 0.35 0.27 0.02 233 1.59 0.02 3.66 2.36 0.17 233 1.71 0.03 3.67 0.71 0.17 233 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.98 0.03 7.61 -0.10 1.34 159 1.28 0.02 553.23 415.07 97.62 269 1.48 0.03 0.41 0.22 0.07 269 1.55 0.02 0.15 0.14 0.03 233 1.59 0.03 3.90 2.00 0.69 233 1.71 0.03 1.41 -0.06 0.25 233 Integration Results for ELS1 A, ELSD SignalLCMS-03 8/16/2018 1:50:21 PM SYSTEMPage1 of4MS Report from Instrument: LCMS-03 RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.36 0.06 33.57 9.70 100.00 269 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.03 0.06 157368.92 42435.76 2.05 159 1.30 0.06 7503950.00 1855827.25 97.95 269LCMS-03 8/16/2018 1:50:21 PM SYSTEMPage2 of4MS Report from Instrument: LCMS-03Ret. Time: 1.03 <<<< POSITIVE SPECTRA >>>> ES-API Positive140001200010000130.280006000102.1400020000100200300400500600700800900m/z161.0159.1168.1280.1279.1199.1233.1258.1Ret. Time: 1.30 ES-API Positive17500015000012500010000075000272.050000250000100200300400500600700800900m/z271.0269.0304.1LCMS-03 8/16/2018 1:50:21 PM SYSTEMPage3 of4MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 8/16/2018 1:50:21 PM SYSTEMPage4 of4