MS Report from Instrument: LCMS-03 File ..MS03\\Data\\20171114\\20171114\\XWJ4843-009-1.D Tgt Mass (CHM): Injection Date : 14 Nov 17 11:38 am +0800 Seq. Line : 41 Sample Name : XWJ4843-009-1 Location : P1-C-10 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\20171114\\20171114\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20171114\\20171114\\1-POS-3MIN.M Catalog No : HY-15893 Batch#27218 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off1.032mAU7501.1981.248250011..9935885000.5530.5880.6700.5 DAD1 B, Sig=254,4 Ref=offmAU1000.58850011.0321.522.5min1.9291.9550.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7020000001500000100000050000000.51 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.70.050-0.05-0.10.5 Integration Results for DAD1 A, Sig=214,4 Ref=off11.0611.522.5min1.522.5min1.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.55 0.02 1.96 1.71 0.13 279 0.59 0.02 2.34 -0.16 0.15 279 0.67 0.02 0.88 0.00 0.06 279 1.03 0.02 1546.66 1168.62 99.33 176 1.20 0.01 0.83 0.85 0.05 176 1.25 0.02 2.45 2.24 0.16 176 1.94 0.01 0.23 0.38 0.01 386 1.96 0.01 1.78 2.21 0.11 386 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.59 0.03 0.91 0.09 0.49 279 1.03 0.02 185.59 138.57 99.15 176 1.93 0.01 0.14 0.17 0.08 386 1.96 0.01 0.53 0.60 0.28 386 Integration Results for MSD1 TIC, MS FileLCMS-03 11/14/2017 13:16:02 SYSTEMPage1 of4MS Report from Instrument: LCMS-03 RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.06 0.07 10032158.00 2267360.50 100.00 176LCMS-03 11/14/2017 13:16:02 SYSTEMPage2 of4MS Report from Instrument: LCMS-03Ret. Time: 1.06 <<<< POSITIVE SPECTRA >>>> ES-API Positive400000350000300000250000200000373.1116.1193.1150000100000500000100200300400500600700800900m/z176.1LCMS-03 11/14/2017 13:16:02 SYSTEMPage3 of4MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 11/14/2017 13:16:02 SYSTEMPage4 of4
